Low pressure combustion process of synthesizing alpha-phase silicon nitride powder |
Title: |
Low pressure combustion process of synthesizing alpha-phase silicon nitride powder |
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Application Number: |
02100183 |
Application Date: |
2002/01/22 |
Announcement Date: |
2002/08/07 |
Pub. Date: |
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Publication Number: |
1362358 |
Announcement Number: |
1173880 |
Grant Date: |
2004-11-3 |
Granted Pub. Date: |
2004-11-3 |
ApplicationType: |
Invention |
State/Country: |
11[China|beijing] |
IPC: |
C01B 21/068, C04B 35/584, C04B 35/64 |
Applicant(s): |
Qinghua Univ. |
Inventor(s): |
Chen Kesi, Zhou Heping, Ge Zhenbin |
Key Words: |
Low pressure combustion, synthesizing, alpha-phase silicon nitride powder |
Abstract: |
The method for synthesizing high alpha-phase silicon nitride powder body by utilizing low-pressure combustion includes the following steps: firstly, pretreating raw material metal silicon powder, according to proportion adding activating agent, diluting agent and additive, ball grinding, fully mixing them, drying, placing them into low-pressure combustion synthesis reaction equipment, evacuating, blowing nitrogen gas into the reaction equipment from bottom, inducing to combustion to implement suspension nitrogenation at low pressure. The purity of said invented product is high, and its alpha-phase content is high. |
Claim: |
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Priority: |
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