Preparation method of polyantimonic acid ion-exchanger |
Title: |
Preparation method of polyantimonic acid ion-exchanger |
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Application Number: |
200610169593 |
Application Date: |
2006/12/22 |
Announcement Date: |
2007/08/01 |
Pub. Date: |
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Publication Number: |
101007290 |
Announcement Number: |
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Grant Date: |
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Granted Pub. Date: |
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ApplicationType: |
Invention |
State/Country: |
11[China|beijing] |
IPC: |
B01J 39/12 |
Applicant(s): |
Tsinghua University |
Inventor(s): |
Li Mingyu, Chen Jing, Wang Jianchen |
Key Words: |
Preparation, polyantimonic acid, ion-exchanger |
Abstract: |
The invention discloses a preparation method of poly-antimonic acid ion exchanger. The method of the invention includes the following steps: 1) antimony trioxide oxidation: antimony trioxide is oxygenated under the presence of oxidants and prepares hydrated antimony pentoxide sol; 2) Oxide aging: aging the prepared hydrated antimony pentoxide sol 1- 30 days under constant temperature of 0 ~ 70 degreeC; 3) drying and exploring in order to form particles: drying the aged hydrated antimony pentoxide sol to poly-antimonic acid solid, putting it into thin nitric acid solution to explore particles and prepares poly-antimonic acid ion exchanger. The invention method has the following advantages: 1. mild preparation conditions and short reaction time; 2. simple installations, low requirements to equipment and easy operation process; 3. preparation process avoids the touch of toxic chemicals; 4. low-cost preparation process, less art operating cost and good adsorption properties of ion exchanger; 5. high selective adsorption capacity of the prepared poly-antimonic acid inorganic ion exchanger to Sr2+. |
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